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العنوان
Characteristic studies of some tetraamine macrocyclic molecules and their chelates with transition metals/
المؤلف
Ali, Naglaa Mashal Mohamed.
هيئة الاعداد
باحث / Naglaa Mashal Mohamed Ali
مناقش / H. A. Dessoky
مشرف / m. E. Moustafa
مشرف / H.M. Ibrahim
الموضوع
Transition metals.
تاريخ النشر
2005.
عدد الصفحات
120 p. ;
اللغة
الإنجليزية
الدرجة
ماجستير
التخصص
Analytical Chemistry
تاريخ الإجازة
1/1/2005
مكان الإجازة
جامعة بنها - كلية العلوم - الكيمياء
الفهرس
Only 14 pages are availabe for public view

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from 186

Abstract

This thesis includes three chapters; the introduction, experimental and results and discussions.
In this chapter, a literature survey of the pervious studies carried out on macrocyclic compounds and their complexes with transition metal ions is given. This survey includes electronic absorption spectra in the UV and visible regions, studies on the metal chelates formed with different transition metal ions, the different techniques of structure elucidation of metal macrocyclic complexes.
This chapter describes the experimental part where it includes the preparation of the Fe(III), Co(II), Ni(II) and Cu(II) macrocyclic complexes by template reaction. It comprises also a description of the instruments used for spectrophotometric, conductometric , IR , thermal analysis, electron spin resonance spectroscopy of Cu(II) complexes, x-ray diffraction, scanning electron microscope, magnetic susceptibility measurements, catalytic studies and electrical conductivity measurements.
This chapter includes the results and discussions and it comprises to three main parts.