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العنوان
Synthesis of Some New Modified Five and Six-Membered Heterocyclic Rings and Their Applications For Silver Ions Recover /
المؤلف
Mansour, Rania El-Araby Mohamed Ead.
هيئة الاعداد
باحث / رانيا العربي محمد عبد منصور
مشرف / عادل عبد الهادي نصار
مناقش / محمد فوده حمزة
مناقش / محمد عبد الله حواطه
الموضوع
organic chemistry.
تاريخ النشر
2023.
عدد الصفحات
173 p. :
اللغة
الإنجليزية
الدرجة
الدكتوراه
التخصص
Organic Chemistry
تاريخ الإجازة
1/5/2023
مكان الإجازة
جامعة المنوفية - كلية العلوم - قسم الكيمياء
الفهرس
Only 14 pages are availabe for public view

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from 173

Abstract

2-thioxodihydropyrimidine-4,6(1H,5H)-dione (1) was obtained by Adding
sodium ethoxide solution, Thiourea and Diethyle malonate. The reaction mixture
was kept reflux in (80%) yield. Scheme 1.
Scheme 1
2,4,6-trichloropyrimidine (2) was obtained by putting 10 ml of
Phospherous oxy chloride for each 1 gm of 1 and reflux it with stiring in (80%)
yield scheme 2
Scheme 2
6-chloropyrimidine-2,4(1H,3H)-dione (3) was obtained by Adding of 2
to NaOH in 30 ml of water and reflux them in (50%) yield, scheme 3.