![]() | Only 14 pages are availabe for public view |
Abstract This work was initiated to obtain a thick carbonitrided layer into the surface of AISI 321 and AISI 316 with high tribological, mechanical and biocombatibility performance. The samples were tested and characterized using X-ray diffraction, optical microscopy, microhardness tester, Form Talysurf 50 profilometer, oscillating ball-on-disk tribometer, contact angle analyzer and Gill AC instrument. Further, in order to preliminary evaluate the biocompatibility performance, bio-tests including blood and cell culture, protein adsorption were applied to the untreated and carbonitrided samples. The current work is classified into two main groups of samples. The first one was devoted to study the effect of rf plasma carbonitriding on the biocompatibility and mechanical properties of AISI 321 austenitic stainless steel. Rf plasma-processing time was varied from 4 to 20 min, while the plasma power was fixed at 500 W. In this study, rf plasma carbonitriding is succeeded to treat the AISI 321 with a high rate of 1.1 μm2/s for plasma-processing time of 8 min. The structural results demonstrate the formation of nitrogen and carbon solid solution phases beside the chromium nitride and iron nitride phases as chemical compounds. The microhardness of the treated layer increased with increasing the processing time to reach a maximum value of 1468 HV0.1 at 16 min. That represents approximately 7-folds increment in the microhardness in comparison with the untreated AISI 321. Further, the wear and corrosion resistance were improved. The friction coefficient decreased from nearly 0.5 for the untreated AISI 321 to nearly 0.25 for the carbonitrided one. Furthermore, .the results reported an agreement |