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Abstract Thesis includes three main chapter I- Introduction The work aimed to prepare and characterize new thiosemicarbazone ligand and its metal complexes aiming to study their effects in the treatment of microbial and tumor diseasesII- Experimental This chapter contains 1) Preparation of thiosemicarbazone ligand and its metal complexes.2) characterization of the ligand and its complexes using:Physical techniques such as molar conductance and magnetic susceptibility Elemental analyses (C, H, N, Cl and M). Spectral techniques as IR, UV- Vis., 1H-NMR, mass spectra and ESR measurements. Thermal analyses (DTA. and TGA)1) Measurement of biological activity |