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Abstract 192 The ,-ray diffractometer with a short wavelength of 77Ir can be used for investigation of crystalline solids. It can expfain the mechanical behaviour (e.g., the stress of silicide film) and the defects of single crystal (e.g., the dislocation). The work in this thesis is classified into two categories by using ,-ray diffractometry as follows: Studying the mechanical behaviour of silicide films: Research within the semiconductor industry on refractory metal silicides has been abundant in recent years. Refractory metal silicides (e.g., TaSi2) have much lower resistivity and have been studied extensively as candidate materials for gate level interconnects for,very large scale integrated circuits (VLSI): During preparation of thin films by evaporation of multilayers (e.g., Si and Ta) or coevaporation, internal or thermal stresses normally arise in the films. The stresses have an important influence on the physical properties of the films. According to the theoretical applications of the ,-ray diffractometry it is possible to obtain the deformation of the lattice planes of the Si substrate. from the rocking curve measurements, it is possible to calculate the radius of curvature of the substrate. Also by different techniques, the thickness of the film can be determined. from these measurements the film stress were calculated. Their investigations were performed as a function of the . |